Microwave Assisted Synthesis of Benzimidazoles From Aromatic Aldehydes
University
Shawnee State University
Major
Chemistry
Presentation Types
Oral Presentation
Keywords:
Benzimidazole, Analytical Chemistry, Microwave
Abstract
Benzimidazoles are an important class of nitrogen containing heterocycles that are found in many natural products, pharmaceuticals, and dyes. A number of benzimidazoles have been synthesized by condensing aromatic aldehydes with various diamines. Many of these compounds exhibit desirable optical properties such as those required for organic dyes, organic LED’s (OLED’s), and dye sensitized solar cells (DSSC’s). Several reports have also shown that such compounds may be useful as chemosensors, specifically as anion sensors. This research focused on developing a concise synthetic procedure using microwave reactor technology in order to efficiently produce highly conjugated benzimidazole systems so that their optical properties could be evaluated. This presentation will report on the progress of new compounds that have been synthesized by reacting ortho, meta, and para phtalaldehydes with various diamines using a CEM Microwave Reactor and an ammonium chloride catalyst. In addition, the subsequent UV–Vis and fluorescence spectroscopic studies of these compounds will be presented.
Faculty Mentor Name
Daniel Finnen
Faculty Mentor Title
Associate Professor of Chemistry
Faculty Mentor Academic Department
Natural Sciences
Recommended Citation
Smith, Dylan, "Microwave Assisted Synthesis of Benzimidazoles From Aromatic Aldehydes" (2019). Celebration of Scholarship. 13.
https://digitalcommons.shawnee.edu/cos/2019/day2/13
Location
LIB 244
Microwave Assisted Synthesis of Benzimidazoles From Aromatic Aldehydes
LIB 244
Benzimidazoles are an important class of nitrogen containing heterocycles that are found in many natural products, pharmaceuticals, and dyes. A number of benzimidazoles have been synthesized by condensing aromatic aldehydes with various diamines. Many of these compounds exhibit desirable optical properties such as those required for organic dyes, organic LED’s (OLED’s), and dye sensitized solar cells (DSSC’s). Several reports have also shown that such compounds may be useful as chemosensors, specifically as anion sensors. This research focused on developing a concise synthetic procedure using microwave reactor technology in order to efficiently produce highly conjugated benzimidazole systems so that their optical properties could be evaluated. This presentation will report on the progress of new compounds that have been synthesized by reacting ortho, meta, and para phtalaldehydes with various diamines using a CEM Microwave Reactor and an ammonium chloride catalyst. In addition, the subsequent UV–Vis and fluorescence spectroscopic studies of these compounds will be presented.